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Beilstein J. Org. Chem. 2010, 6, No. 30, doi:10.3762/bjoc.6.30
Graphical Abstract
Scheme 1: Synthesis of 1 and 3. (a) Pyridazine, toluene, reflux, 20 h; (b) NaI, DMF, 65 °C, 15 h.
Scheme 2: Synthesis of 2 and 4. (a) NaI, DMF, 65 °C, 24 h; (b) AgSbF6, THF.
Figure 1: ORTEP drawing of the crystal structures: a) 2 and b) 3. For additional perspective representations ...
Figure 2: a) ORTEP drawing of the crystal structure of 4. Ag+ and Ag+, describe the two disordered positions ...
Scheme 3: Synthesis of 5 and 6. (a) Toluene, 90 °C, 15 h.
Figure 3: ORTEP drawing of the crystal structures: a) 5b and b) 6. For additional perspective representations...